1-((1R)-((2R,4R,5S)-5-ethylquinuclidin-2-yl)(6-methoxyquinolin-4-yl)methoxy)-4-((1R)-((2R,4S,5R)-5-ethylquinuclidin-2-yl)(6-methoxyquinolin-4-yl)methoxy)phthalazine → HCID 54767677, compound

Participants

Reaction Steps

Compound 141 (white solid) was prepared following the procedure described for preparing compound 139 using Ad-mix-α instead of Ad-mix-β: 1H-NMR (400 MHz, CD3OD): δ 7.82 (d, 1H, 8.8 Hz), 7.53-7.57 (m, 3H), 7.34-7.39 (m, 2H), 7.31 (s, 1H), 7.23-7.27 (m, 3H), 7.1-7.14 (m, 1H), 5.44-5.51 (m, 1H), 3.89-3.95 (m, 1H), 3.72-3.76 (m, 1H), 3.47-3.63 (m, 3H), 3.12-3.18 (m, 1H), 2.86-2.97 (m, 1H); LC/MS: m/z=535.2 [M+Na]+ (Calc: 512.5).

Provenance & Evidence