HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-methylpropyn-2-ylamine → Benzyl 2-(3-(methyl(prop-2-ynyl)amino)oxetan-3-yl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-methylpropyn-2-ylamine | HCID 96160 | — |
| Reactant | Benzyl (oxetan-3-ylidene)acetate | HCID 54759148 | — |
| Product | Benzyl 2-(3-(methyl(prop-2-ynyl)amino)oxetan-3-yl)acetate | HCID 86663091 | — |
Reaction Steps
A mixture of N-methyl-propargylamine (0.27 g) and benzyl 2-(oxetan-3-ylidene)acetate (0.41 g) was stirred neat at RT for 12 h. The excess amine was removed by evaporation to give benzyl 2-(3-(methyl(prop-2-ynyl)amino)oxetan-3-yl)acetate quantitatively (0.54 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09212175B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-2412ee43c72e4dc59f52343124b808f4 |
| Source note | uspto-grants-2015_12 |