HCID 86725381, compound → HCID 86725382, compound

Participants

Reaction Steps

A mixture of the product of Example 16C (560 mg, 1.1 mmol) and 10% palladium on carbon in methanol (30 mL) was stirred at ambient temperature under hydrogen until TLC indicated no starting material remained. The mixture was filtered through diatomaceous earth and the filtrate was concentrated. The residue was purified by flash chromatography on silica gel (200-300 mesh) eluting with 4/1 petroleum ether/ethyl acetate to give the title compound. MS: 314 (M+H+),

Provenance & Evidence