HRID1503891

反应详情

EQUATION

反应方程式

HRID 1503891 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a mixture of 10% palladium on carbon (0.1 g) in methanol (30 mL) was added the product of Example 62A (0.8 g, 2.6 mmol) and the mixture was stirred at ambient temperature under hydrogen for 8 hours. The mixture was filtered and concentrated to yield the title compound. MS: 307 (M+H+).

WORKUP

后处理

  1. filtrationThe mixture was filtered
  2. concentrationconcentrated