HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Butyldiethanolamine → 6-Butyl-1,3,6-dioxazocan-2-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Butyldiethanolamine | HCID 7620 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | 6-Butyl-1,3,6-dioxazocan-2-one | HCID 118380294 | 239.2% |
Reaction Steps
The procedure of Example 1 was followed using N-butyl diethanolamine (13.5 g, 83.9 mmol), triethylamine (24.0 mL, 167.8 mmol), dry THF (600 mL) and triphosgene (8.3 g, 28.8 mmol). The filtrate was concentrated yielding a yellow/brown oil product (12.9 g, 82%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09215876B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-24c0c767132642f883f7580d4bab7314 |
| Source note | uspto-grants-2015_12 |