HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,2'-((Phenylmethyl)imino)bisethanol → HCID 118380279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,2'-((Phenylmethyl)imino)bisethanol | HCID 7553 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 118380279 | HCID 118380279 | 227.6% |
Reaction Steps
The procedure of Example 1 was followed using N-benzyl diethanolamine (16.4 g, 83.9 mmol), triethylamine (24.0 mL, 167.8 mmol), dry THF (600 mL) and triphosgene (8.3 g, 28.8 mmol). The filtrate was concentrated yielding a yellow oil product (14.5 g, 78%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09215876B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-3d51acbbf6bd4a9ea2713b6ee202d806 |
| Source note | uspto-grants-2015_12 |