HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylene Glycol → HCID 57841306, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylene Glycol | HCID 8117 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Triphosgene | HCID 94429 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57841306 | HCID 57841306 | — |
Reaction Steps
The procedure of Example 1 was followed using diethylene glycol (8.9 g, 83.9 mmol), triethylamine (24.0 mL, 167.8 mmol), dry THF (600 mL) and triphosgene (8.3 g, 28.8 mmol). The filtrate was concentrated yielding only oligomeric compounds.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09215876B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-df35ce2d1d7e4751a6644dc73910359c |
| Source note | uspto-grants-2015_12 |