Thiodiglycol → HCID 118380274, compound

Participants

Reaction Steps

The procedure of Example 1 was followed using 2,2′-thiodiethanol (10.2 g, 83.9 mmol), triethylamine (24.0 mL, 167.8 mmol), dry THF (600 mL) and triphosgene (8.3 g, 28.8 mmol). The filtrate was concentrated yielding only oligomeric compounds.

Provenance & Evidence