Dimethylformamide → HCID 71617343, compound

Participants

Reaction Conditions

Reaction Steps

6-[(E)-2-(5,8-Dimethyl-[1,2,4]triazolo[1,5-a]pyrazin-2-yl)-vinyl]-1,3-dioxolo[4,5-g]quinoline (0.183 g, 0.530 mmol) was dissolved in N,N-Dimethylformamide (11 mL, 140 mmol). [B] p-Toluenesulfonylhydrazide (0.296 g, 1.59 mmol; Supplier=Avocado) was added and the reaction was stirred at 130° C. under an atmosphere of Argon ON. LCMS was done and showed almost complete conversion. 0.100 g [B] was added to the mixture was stirred 2 days at 130 C.

Provenance & Evidence