Thionyl Chloride → HCID 71715030, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of 5-phenethyl-6-(trifluoromethyl)-2,3,5,6-tetrahydro-[1,4]oxazino[2,3,4-hi]indol-6-ol (208 mg, 0.60 mmol) in pyridine (3 mL) was added thionyl chloride (142 mg, 1.2 mmol) at 0° C. After stirring for 2 h at 0° C., the resulting mixture was concentrated to yield 5-phenethyl-6-(trifluoromethyl)-2,3-dihydro-[1,4]oxazino[2,3,4-hi]indole.

Provenance & Evidence