HCID 90229228, compound → HCID 90229616, compound

Participants

Reaction Steps

To a solution of methyl 5-{[(benzyloxy)carbonyl]amino}-1-{[2-(trimethylsilyl)ethoxy]methyl}-1H-indazole-7-carboxylate (364 mg) in MeOH (10 mL) was added 5% palladium on carbon (55 mg), and the reaction mixture was stirred overnight under hydrogen atmosphere at an ordinary pressure. The reaction mixture was filtered off on celite and washed with MeOH. The mother liquor was concentrated under reduced pressure to obtain the titled compound (234 mg) as green powder.

Provenance & Evidence