2,4-Di-tert-butylphenol → HCID 19001508, compound

HRID 1506084Notes

Reaction equation

HRID 1506084 reaction equation
[C:1]([C:5]1[CH:10]=[C:9](C(C)(C)C)[CH:8]=[CH:7][C:6]=1[OH:15])(C)(C)[CH3:2].C(OC[N:22](COCC(C)C)C)C(C)C>C1(C)C=CC=CC=1>[O:15]1[C:6]2=[CH:7][CH:8]=[CH:9][CH2:10][CH:5]2[CH2:1][CH2:2][NH:22]1

Participants

4

Reactant 2

HCID 73112,4-Di-tert-butylphenolHCID 21821394HCID 21821394, compound

Product 1

HCID 19001508HCID 19001508, compoundYield 189.8%

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Conditions

Temperature
80 °C

Procedure

A 1000 ml four-neck flask was initially charged with 206 g of 2,4-di-tert-butylphenol at room temperature in 400 ml of toluene. 203 g of N,N-di(isobutoxymethyl)-N-methylamine from example 1 were added rapidly. The flask contents were stirred at 80° C. for 60 minutes. The solution was concentrated by evaporation at 120° C. and 5 mbar. 260 g of product were obtained.

Workup

  1. concentrationThe solution was concentrated by evaporation at 120° C.

Sources & evidence

ORD record
ord-026c0439dd5d40e89f6d9741ee0b2c46
Source dataset
uspto-grants-2015_12
Patent number
US09217115B2

Reaction notes

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