HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 136341311, compound → HCID 178520936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 136341311 | HCID 136341311 | — |
| Reactant | HCID 178455224 | HCID 178455224 | — |
| Product | HCID 178520936 | HCID 178520936 | 78% |
Reaction Steps
The reactions in Synthetic Examplea 140 were carried out in substantially the same manners except that 1-(trans-4-{[(tert-butyldimethylsilyl)oxy]methyl}cyclohexyl)-7H-pyrrolo[3,2-e][1,2,3]triazolo[1,5-c]pyrimidine obtained in Reference Synthetic Examplea 92 was used instead of 1-(4-{[(tert-butyldimethylsilyl)oxy]methyl}phenyl)-7H-pyrrolo[3,2-e][1,2,3]triazolo[1,5-c]pyrimidine to give the title compound as a pale yellow solid (2.05 g, yield 78%). (alternative to Synthetic Examplea 10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09216999B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-cea2577091d24810bc0cb7a9002e3e58 |
| Source note | uspto-grants-2015_12 |