Dibutadiamine → HCID 71471615, compound

HRID 1506754Notes

Reaction equation

[Cl:1][C:2]1[CH:3]=[C:4]2[C:13](=[CH:14][CH:15]=1)[C:12](Cl)=[C:11]1[C:6]([CH:7]=[CH:8][C:9]([O:17][CH3:18])=[CH:10]1)=[N:5]2.[C:19]([NH:23][CH2:24][CH2:25][CH2:26][CH2:27][NH2:28])([CH3:22])([CH3:21])[CH3:20]>>[C:19]([NH:23][CH2:24][CH2:25][CH2:26][CH2:27][NH:28][C:12]1[C:13]2[C:4]([N:5]=[C:6]3[C:11]=1[CH:10]=[C:9]([O:17][CH3:18])[CH:8]=[CH:7]3)=[CH:3][C:2]([Cl:1])=[CH:15][CH:14]=2)([CH3:22])([CH3:21])[CH3:20]

Participants

Reactant 2

HCID 15853Dibutadiamine

HCID 665773,9-Dichloro-7-methoxyacridine

Product 1

HCID 71471615HCID 71471615, compound

Procedure

Following the general procedure of Example 1 and making non-critical variations, but using 6,9-dichloro-2-methoxyacridine and commercially available N1-tert-butylbutane-1,4-diamine, the title compound was obtained; MS (Found M+1=386).

Sources & evidence

ORD record: ord-671d3c54168b4bb7ac2aa0a125057425
Source dataset: uspto-grants-2015_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US09221760B2

Reaction notes

Loading…