HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromobenzoic acid → HCID 71656518, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromobenzoic acid | HCID 11464 | — |
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 4-Bromobenzoyl chloride | HCID 68515 | — |
| Reactant | N-(2-Butyl-1-benzofuran-5-yl)methanesulfonamide | HCID 9878493 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71656518 | HCID 71656518 | — |
Reaction Steps
5.08 g of 4-bromobenzoyl chloride—prepared by reacting 4-bromobenzoic acid with thionyl chloride—and 5.42 g of 2-butyl-5-methanesulfonamido-benzofuran (IV) were dissolved in 30 ml of dichloromethane. The reaction was performed according to Example 10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221777B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-34c0651bca114ad693992d57361e9623 |
| Source note | uspto-grants-2015_12 |