HCID 68278814, compound → HCID 56961289, compound
Reaction equation
[C:1]1([S:7]([NH:10][C:11]2[S:19][C:18]3[CH2:17][CH2:16][O:15][CH2:14][C:13]=3[C:12]=2[C:20]([O:22]C)=[O:21])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.C1(S(N(S(C2C=CC=CC=2)(=O)=O)C2SC3CCOCC=3C=2C(OC)=O)(=O)=O)C=CC=CC=1>>[C:1]1([S:7]([NH:10][C:11]2[S:19][C:18]3[CH2:17][CH2:16][O:15][CH2:14][C:13]=3[C:12]=2[C:20]([OH:22])=[O:21])(=[O:8])=[O:9])[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1Participants
3
Procedure
Prepared by proceeding in a similar manner to Example 2, starting from a mixture of methyl 2-benzenesulphonylamino-6,7-dihydro-4H-thieno[3,2-c]pyran-3-carboxylate and methyl 2-[bis-(benzenesulphonyl)amino]-6,7-dihydro-4H-thieno[3,2-c]pyran-3-carboxylate (Intermediate 14)
Workup
- customPrepared
Sources & evidence
- ORD record
- ord-86ffa286a66f47fcb947022d6c10d3d5
- Source dataset
- uspto-grants-2015_12
- Patent number
- US09221787B2
Reaction notes
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