HCID 68278836, compound → HCID 56961399, compound

HRID 1506896Notes

Reaction equation

HRID 1506896 reaction equation
[F:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:11][C:12]2[S:16][C:15]3[CH2:17][CH2:18][CH2:19][CH2:20][C:14]=3[C:13]=2[C:21]([O:23]CC)=[O:22])(=[O:10])=[O:9])=[C:4]([CH3:26])[CH:3]=1.FC1C=CC(S(N(S(C2C=CC(F)=CC=2C)(=O)=O)C2SC3CCCCC=3C=2C(OCC)=O)(=O)=O)=C(C)C=1>>[F:1][C:2]1[CH:7]=[CH:6][C:5]([S:8]([NH:11][C:12]2[S:16][C:15]3[CH2:17][CH2:18][CH2:19][CH2:20][C:14]=3[C:13]=2[C:21]([OH:23])=[O:22])(=[O:10])=[O:9])=[C:4]([CH3:26])[CH:3]=1

Participants

3

Reactant 2

HCID 68278836HCID 68278836, compoundHCID 86693762HCID 86693762, compound2×

Product 1

HCID 56961399HCID 56961399, compound

Procedure

Prepared by proceeding in a similar manner to Example 2, starting from a 2:1 mixture of ethyl 2-(4-fluoro-2-methylbenzenesulphonylamino)-4,5,6,7-tetrahydro-benzo[b]thiophene-3-carboxylate and ethyl 2-[bis-(4-fluoro-2-methyl-benzenesulphonyl)amino]-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate (Intermediate 32)

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-d3f375dda78a44abb7aafa6aed63520d
Source dataset
uspto-grants-2015_12
Patent number
US09221787B2

Reaction notes

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