Ethyl 2-(benzenesulfonamido)-4,5,6,7-tetrahydrobenzothiophene-3-carboxylate → HCID 68278699, compound
Reaction equation
[C:1]1([S:7]([NH:10][C:11]2[S:15][C:14]3[CH2:16][CH2:17][CH2:18][CH2:19][C:13]=3[C:12]=2[C:20]([O:22][CH2:23][CH3:24])=[O:21])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:25][O:26]C1C=C(S(Cl)(=O)=O)C=CC=1>>[CH3:25][O:26][C:5]1[CH:6]=[C:1]([S:7]([NH:10][C:11]2[S:15][C:14]3[CH2:16][CH2:17][CH2:18][CH2:19][C:13]=3[C:12]=2[C:20]([O:22][CH2:23][CH3:24])=[O:21])(=[O:9])=[O:8])[CH:2]=[CH:3][CH:4]=1Participants
3
Procedure
Prepared by proceeding in a similar manner to Intermediate 1, starting from ethyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxlyate and 3-methoxybenzenesulphonyl chloride.
Workup
- customPrepared
Sources & evidence
- ORD record
- ord-bbcc1dd8381a46efbe37536703fd2a47
- Source dataset
- uspto-grants-2015_12
- Patent number
- US09221787B2
Reaction notes
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