Benzenesulfonyl chloride → HCID 68278813, compound

HRID 1506926Notes

Reaction equation

HRID 1506926 reaction equation
[C:1]1([S:7]([NH:10][C:11]2[S:15][C:14]3C[CH2:17][CH2:18][CH2:19][C:13]=3[C:12]=2[C:20]([O:22][CH2:23][CH3:24])=[O:21])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.NC1SC2CCCC=2C=1C(OCC)=O.C1(S(Cl)(=O)=O)C=CC=CC=1>>[C:1]1([S:7]([NH:10][C:11]2[S:15][C:14]3[CH2:17][CH2:18][CH2:19][C:13]=3[C:12]=2[C:20]([O:22][CH2:23][CH3:24])=[O:21])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 3

HCID 7369Benzenesulfonyl chlorideHCID 264105ethyl 2-amino-4H,5H,6H-cyclopenta[b]thiophene-3-carboxylateHCID 391240Ethyl 2-(benzenesulfonamido)-4,5,6,7-tetrahydrobenzothiophene-3-carboxylate

Product 1

HCID 68278813HCID 68278813, compound

Procedure

Prepared by proceeding in a similar manner to Intermediate 1, starting from ethyl 2-amino-5,6-dihydro-4H-cyclopenta[b]thiophene-3-carboxylate and benzenesulphonyl chloride.

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-f070b4f9748043b7bd6f3c2b2a745508
Source dataset
uspto-grants-2015_12
Patent number
US09221787B2

Reaction notes

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