4-Chlorobenzenesulfonyl chloride → HCID 3941347, compound

HRID 1506927Notes

Reaction equation

HRID 1506927 reaction equation
[C:1]1([S:7]([NH:10][C:11]2[S:15][C:14]3[CH2:16][CH2:17][CH2:18][CH2:19][C:13]=3[C:12]=2[C:20]([O:22][CH2:23]C)=[O:21])(=[O:9])=[O:8])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.NC1SC2CCCCC=2C=1C(OC)=O.[Cl:39]C1C=CC(S(Cl)(=O)=O)=CC=1>>[Cl:39][C:4]1[CH:5]=[CH:6][C:1]([S:7]([NH:10][C:11]2[S:15][C:14]3[CH2:16][CH2:17][CH2:18][CH2:19][C:13]=3[C:12]=2[C:20]([O:22][CH3:23])=[O:21])(=[O:9])=[O:8])=[CH:2][CH:3]=1

Participants

4

Reactant 3

HCID 73984-Chlorobenzenesulfonyl chlorideHCID 391240Ethyl 2-(benzenesulfonamido)-4,5,6,7-tetrahydrobenzothiophene-3-carboxylateHCID 2756552Methyl 2-amino-4,5,6,7-tetrahydro-1-benzothiophene-3-carboxylate

Product 1

HCID 3941347HCID 3941347, compound

Procedure

Prepared by proceeding in a similar manner to Intermediate 1, starting from methyl 2-amino-4,5,6,7-tetrahydrobenzo[b]thiophene-3-carboxylate and 4-chlorobenzene-sulphonyl chloride

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-07b4fc8fbddd447e816f70ad6281a230
Source dataset
uspto-grants-2015_12
Patent number
US09221787B2

Reaction notes

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