HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromoacetonitrile → HCID 90375094, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromoacetonitrile | HCID 11534 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | HCID 90375134 | HCID 90375134 | — |
| Product | HCID 90375094 | HCID 90375094 | — |
Reaction Steps
By General Procedure T from tert-butyl N-{[4-(aminomethyl)pyridin-2-yl]methyl}-N-{4-[benzyl(cyclopropyl)amino]butyl}carbamate (1 equiv.) and bromoacetonitrile (1.1 equiv.), using 2 equiv. DIPEA. Aqueous work up gave the title product, which was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221801B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-c07c1059ad364468aa72a820725ea998 |
| Source note | uspto-grants-2015_12 |