HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-formylpyridine-4-carboxylate → ethyl 2-(((2-((2-(dimethylamino)ethyl)(ethyl)amino)-2-oxoethyl)amino)methyl)isonicotinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-formylpyridine-4-carboxylate | HCID 19600808 | — |
| Reactant | HCID 90093426 | HCID 90093426 | — |
| Product | ethyl 2-(((2-((2-(dimethylamino)ethyl)(ethyl)amino)-2-oxoethyl)amino)methyl)isonicotinate | HCID 90094283 | — |
Reaction Steps
By General Procedure A from ethyl 2-formylpyridine-4-carboxylate and 2-amino-N-[2-(dimethylamino)ethyl]-N-ethylacetamide. 1H NMR (300 MHz, CDCl3), δ ppm: 3.47-3.32 (m, 4H), 3.27-3.20 (m, 2H), 2.44-2.35 (m, 2H), 2.22 (s, 6H), 1.53 (s, 2H), 1.15-1.06 (m, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221801B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-a71e15c6533d41a7a1669c406301a3ff |
| Source note | uspto-grants-2015_12 |