HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 2-formylpyridine-4-carboxylate → HCID 90374998, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 2-formylpyridine-4-carboxylate | HCID 19600808 | — |
| Reactant | HCID 21843884 | HCID 21843884 | — |
| Product | HCID 90374998 | HCID 90374998 | — |
Reaction Steps
By General Procedure A from ethyl 2-formylpyridine-4-carboxylate and {4-[(dimethylamino)methyl]cyclohexyl}methanamine. Aqueous work up gave the title compound as a yellow oil. Used without further purification. 1H NMR (300 MHz, chloroform-d): δ ppm 8.41 (d, 1H), 8.04 (s, 1H), 7.49 (d, 1H), 4.04 (q, 2H), 3.39 (s, 2H), 2.46 (m, 4H), 2.38 (d, 6H), 1.60 (m, 4H), 1.34 (t, 3H), 1.03 (m, 2H), 0.68 (m, 4H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221801B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-a32ef5bcf602421a8c13474aa62f62c3 |
| Source note | uspto-grants-2015_12 |