HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methyl-4-methoxycarbonylphenylboronic acid, pinacol ester → HCID 57407160, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methyl-4-methoxycarbonylphenylboronic acid, pinacol ester | HCID 11087024 | — |
| Reactant | 2-Chloro-6-methoxyquinazoline | HCID 59254852 | — |
| Product | HCID 57407160 | HCID 57407160 | — |
Reaction Steps
Prepared according to Scheme 6, B conditions, starting from Intermediate 8 and methyl 3-methyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate. 1H NMR (DMSO-d6 400 MHz): δ 9.54 (s, 1H), 8.00-7.86 (m, 4H), 7.60 (dd, J=8.8, 2.4 Hz, 1H), 7.36 (d, J=2.4 Hz, 1H), 2.59 (s, 3H). MS (ESI): m/z 280.9[M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221810B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-92654e6d368f43df9b694b3ddb08e208 |
| Source note | uspto-grants-2015_12 |