Morpholinoamidine → HCID 178517897, 화합물

참여 물질

반응 단계

A mixture 1,3-diethyl 2-(1,3-benzothiazol-2-yl)propanedioate (3.00 g, 10.23 mmol, 1.00 equiv), and morpholine-4-carboximidamide (1.33 g, 10.30 mmol, 1.00 equiv) in Toluene (30 mL) was heated for 20 h at 120° C. under an inert atmosphere of nitrogen. After cooling down, the white solid was collected by filtration, washed with a mixture solution of Dichloromethane/Methanol and dried in an IR oven to afford the title compound. as a white solid. MS m/z [M+H]+ (ESI): 331.

출처 및 근거