3-Pyridinecarbonyl chloride, hydrochloride (1:1) → HCID 73426646, compound

HRID 1507603Notes

Reaction equation

HRID 1507603 reaction equation
Cl.[NH2:2][C:3]1[N:8]=[C:7]2[N:9]([CH3:15])[C:10](=[O:14])[C:11]([CH3:13])([CH3:12])[C:6]2=[CH:5][CH:4]=1.Cl.[C:17](Cl)(=[O:24])[C:18]1[CH:23]=[CH:22][CH:21]=[N:20][CH:19]=1>>[CH3:15][N:9]1[C:7]2=[N:8][C:3]([NH:2][C:17](=[O:24])[C:18]3[CH:23]=[CH:22][CH:21]=[N:20][CH:19]=3)=[CH:4][CH:5]=[C:6]2[C:11]([CH3:12])([CH3:13])[C:10]1=[O:14]

Participants

3

Reactant 2

HCID 884383-Pyridinecarbonyl chloride, hydrochloride (1:1)HCID 90047521HCID 90047521, compound

Product 1

HCID 73426646HCID 73426646, compound

Procedure

Prepared in analogy to example 2 using 6-amino-1,3,3-trimethyl-1H-pyrrolo[2,3-b]pyridin-2-one hydrochloride (example 76c) and nicotinoyl chloride hydrochloride. The title compound was obtained as light yellow solid.

Sources & evidence

ORD record
ord-b78ceabb255845aa8a2f7f0deae9fecf
Source dataset
uspto-grants-2015_12
Patent number
US09221816B2

Reaction notes

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