huagongshe.com
HRID1507770

反应详情

EQUATION

反应方程式

HRID 1507770 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)CCOc1ccc(F)cc1
HCID74099

3-(4-Fluorophenoxy)propionic acid

C9H9FO3

结构：COC(=O)C(N)C(=O)OC
HCID437601

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C(NC(=O)CCOc1ccc(F)cc1)C(=O)OC
HCID50941576

未命名化合物

收率 80%

PROCEDURE

实验过程

This compound was synthesized from dimethyl aminomalonate according to the procedure for the preparation of example 2 using 3-(4-fluorophenoxy)propionic acid. The crude residue was purified by flash chromatography on silica (CH2Cl2/MeOH 50:1) to yield the title compound as a white solid (80%).

WORKUP

后处理

  1. customThe crude residue was purified by flash chromatography on silica (CH2Cl2/MeOH 50:1)