HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorophenethyl Alcohol → 2-(4-Fluorophenyl)acetaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorophenethyl Alcohol | HCID 82068 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-(4-Fluorophenyl)acetaldehyde | HCID 11126322 | — |
Reaction Steps
To a stirred suspension of pyridinium chlorochromate (6.9 g, 21.4 mmol) in CH2Cl2 (100 ml) was added a solution of 2-(4-fluorophenyl)ethanol (3.0 g, 21.4 mmol) in CH2Cl2 (10 ml). The resulting suspension was stirred for 2 hours at room temperature and was then diluted with ether. The resulting suspension was filtered through a pad of Celite and washed with ether.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221822B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-cfdb1201d7f1469fbca4d1afd4eb2ec3 |
| Source note | uspto-grants-2015_12 |