6-Methyl-furo[2,3-B]pyridin-3-one → 6-methylfuro[2,3-b]pyridin-3(2H)-one O-methyl oxime

Participants

Reaction Steps

This compound was prepared using a method analogous to that of furo[2,3-c]pyridazin-5(6H)-one O-methyl oxime (A.2.3.3), 6-methylfuro[2,3-b]pyridin-3(2H)-one replacing furo[2,3-c]pyridazin-5(6H)-one. Purification by (KP-SIL™ from Biotage) using Hept to Hept/EtOAc (1/1) gives the desired product as white solid;

Provenance & Evidence