HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bis(neopentyl glycolato)diboron → HCID 86704608, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bis(neopentyl glycolato)diboron | HCID 2734316 | — |
| Reactant | 4-(4-Methoxyphenyl)cyclohexanone | HCID 10976581 | — |
| Reactant | 3-(4-Methoxyphenyl)cyclopentan-1-one | HCID 14090910 | — |
| Reactant | HCID 86704609 | HCID 86704609 | — |
| Product | HCID 86704608 | HCID 86704608 | — |
Reaction Steps
The title compound was synthesized from 3-(4-methoxyphenyl)cyclopentanone (INTERMEDIATE 75, Step B) and commercially available starting materials using an analogous method to that described for INTERMEDIATE 7. Bis(neopentyl glycolato)diboron was used instead of BISPIN to afford a mixture of the titled compound and methyl (1S,3R)-3-[3-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)-4-methoxyphenyl]cyclopentanecarboxylate. The mixture was used without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221834B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-1fc2d19e43c2436d861550b7ab2c5426 |
| Source note | uspto-grants-2015_12 |