HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Aminophenylacetic acid ethyl ester → HCID 90338516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Aminophenylacetic acid ethyl ester | HCID 225219 | — |
| Reactant | HCID 90111594 | HCID 90111594 | — |
| Product | HCID 90338516 | HCID 90338516 | 78% |
Reaction Steps
Following general procedure H, 2-(3-chlorophenyl)-5,5-dioxido-7,8-dihydro-6H-thiopyrano[3,2-d]pyrimidin-4-yl trifluoromethanesulfonate (1.0 g, 2.26 mmol) was reacted with ethyl 2-(4-aminophenyl)acetate (0.445 g, 2.49 mmol) to afford the title compound (0.827 g, 78%) as a light yellow solid. MW=471.96. APCI MS m/z 472 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221843B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-ff4c91487554446894ca685581299608 |
| Source note | uspto-grants-2015_12 |