HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-methoxy-N-(4-methoxybutyl)-2-nitroaniline → 6-Methoxy-2-(4-methoxybutylamino)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-methoxy-N-(4-methoxybutyl)-2-nitroaniline | HCID 58355768 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 6-Methoxy-2-(4-methoxybutylamino)aniline | HCID 58355726 | 103.5% |
Reaction Steps
3-Methoxy-N-(4-methoxybutyl)-2-nitroaniline (230 mg) was dissolved in methanol (30 ml), palladium-carbon (5%, 90 mg) was added, and the mixture was stirred for 2 hr under a hydrogen atmosphere. The reaction mixture was filtered through celite, and the filtrate was concentrated under reduced pressure to give the object product (210 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09221836B2 |
| Source dataset | uspto-grants-2015_12 |
| ORD ID | ord-b25f06d14d434680a6ee846eb580dad4 |
| Source note | uspto-grants-2015_12 |