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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1509596Generated: October 29, 2026

Hydrogen chloride-ethyl acetate → HCID 67321792, compound

https://huagongshe.com/reaction/1509596

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrogen chloride-ethyl acetateHCID 21866389—
ReactantHCID 58355330HCID 58355330—
SolventEthyl AcetateHCID 8857—
ProductHCID 67321792HCID 67321792—

Reaction Steps

tert-Butyl (3S,5R)-3-[{[1-(4-methoxybutyl)-5-phenyl-1H-pyrrol-2-yl]carbonyl}(2-methylpropyl)amino]-5-(morpholin-4-ylcarbonyl)piperidine-1-carboxylate (150 mg) was dissolved in ethyl acetate (5 ml), 4N hydrogen chloride-ethyl acetate (5 ml) was added and the mixture was stirred for 1 hr. The solvent was evaporated under reduced pressure to give the object product (110 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09221836B2
Source datasetuspto-grants-2015_12
ORD IDord-280826279ae54e37a95a139ee30b9faf
Source noteuspto-grants-2015_12