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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1509796Generated: October 31, 2026

Potassium Carbonate → HCID 68495665, compound

https://huagongshe.com/reaction/1509796

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
Reactant1-MethylpiperazineHCID 53167—
ReactantHCID 25126264HCID 25126264—
SolventDimethyl SulfoxideHCID 679—
ProductHCID 68495665HCID 68495665—

Reaction Conditions

Temperature90 °C

Reaction Steps

0.31 g (0.0030 mol) of N-methylpiperazine was added to the mixture of 0.41 g (0.015 mol) of 2-(2′-nitro-5′-fluorophenyl)benzothiazole and 0.32 g (0.0023 mol) of K2CO3 in 5 ml of dimethyl sulfoxide. The reaction was stirred magnetically and heated at 90° C., the progression thereof being verified by TLC.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08211662B2
Source datasetuspto-grants-2012_07
ORD IDord-2dfc2ce301f24088acdd8e062b4dee75
Source noteuspto-grants-2012_07