HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminosalicylic Acid → HCID 7027806, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminosalicylic Acid | HCID 4075 | — |
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Product | HCID 7027806 | HCID 7027806 | 56% |
Reaction Steps
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (500 mg, 3.26 mmole) and 4-nitrobenzoyl chloride (700 mg, 3.77 mmole), 550 mg (56% yield) of 5-(4-nitrobenzoyl)aminosalicylic acid was obtained as a pale yellow solid.:mp 270-271° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211877B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-34982c6e4a4245bd80235e1a7fb451f0 |
| Source note | uspto-grants-2012_07 |