HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Aminosalicylic Acid → HCID 9943418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Aminosalicylic Acid | HCID 4075 | — |
| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Product | HCID 9943418 | HCID 9943418 | 50% |
Reaction Steps
By following the similar procedure in Synthesis Example 1 by using 5-aminosalicylic acid (1.00 g, 6.53 mmole) and 4-methoxybenzyl chloride (1.23 g, 7.84 mmole), 890 mg (50% yield) of 5-(4-methoxybenzyl)aminosalicylic acid was obtained as a white solid.: mp 205-206° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211878B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-d828dadede9f4b2bbdea020f47abd506 |
| Source note | uspto-grants-2012_07 |