HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-nitroaniline → 3,5-dichloro-N-(2-chloro-4-nitrophenyl)-2-hydroxybenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-nitroaniline | HCID 8492 | — |
| Reactant | 3,5-Dichlorosalicylic acid | HCID 9445 | — |
| Product | 3,5-dichloro-N-(2-chloro-4-nitrophenyl)-2-hydroxybenzamide | HCID 2946176 | — |
Reaction Steps
This material was prepared according to the method of Example 1 using 3,5-dichlorosalicylic acid and 2-chloro-4-nitroaniline, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ7.85 (m, 1H, H4), 7.98 (m, 1H, H5), 8.29 (m, 1H, H5′), 8.04 (m, 1H, H6), 8.44 (m, 1H, H3′), 8.55 (m, 1H, H6′).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211882B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-46521701bd6a429db9f8176d19f5783f |
| Source note | uspto-grants-2012_07 |