HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorosalicylic Acid → HCID 44241054, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorosalicylic Acid | HCID 9447 | — |
| Reactant | 3-Aminostyrene | HCID 4260041 | — |
| Product | HCID 44241054 | HCID 44241054 | — |
Reaction Steps
This material was prepared according to the method of Example 1 using 5-chlorosalicylic acid and 3-vinylaniline, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ 5.32 (m, 1H, C═CH2 cis), 5.83 (m, 1H, C═CH2 trans), 6.75 (m, 1H, ArCH═CH2), 7.02 (m, 1H, H3), 7.28 (m, 1H, H6′), 7.37 (m, 1H, H5′), 7.49 (m, 1H, H4), 7.62 (m, 1H, H4′), 7.80 (m, 1H, H2′), 7.90 (m, 1H, H6).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211882B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-1138927c0071470bb1cca45892935314 |
| Source note | uspto-grants-2012_07 |