HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chlorosalicylic Acid → 5-Chloro-2-hydroxy-N-(3-methoxyphenyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chlorosalicylic Acid | HCID 9447 | — |
| Reactant | 3-Methoxyaniline | HCID 10824 | — |
| Product | 5-Chloro-2-hydroxy-N-(3-methoxyphenyl)benzamide | HCID 18104278 | — |
Reaction Steps
This material was prepared according to the method of Example 1 using 5-chlorosalicylic acid and m-anisidine, with reagents and solvents employed in similar molar ratios. 1HNMR (500 MHz, DMSO-d6): δ 3.72 (s, 3H), 6.74 (m, 1H), 7.09 (m, 1H), 7.26 (br m, 2H), 7.40 (br s, 1H), 7.47 (m, 1H), 7.88 (m, 1H), 10.34 (s, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211882B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-f35e4eb15faf4b21944933ddd46ed0c3 |
| Source note | uspto-grants-2012_07 |