HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-8-(trifluoromethyl)quinoline → HCID 59590549, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-8-(trifluoromethyl)quinoline | HCID 90262 | — |
| Reactant | 6-Hydroxy-1-naphthoic acid | HCID 5463800 | — |
| Product | HCID 59590549 | HCID 59590549 | 49.1% |
Reaction Steps
The title compound (1.43 g, 49% yield) was prepared as a brown solid from 6-hydroxy-1-naphthoic acid (1.43 g, 7.6 mmol) and 4-chloro-8-(trifluoromethyl)quinoline (2.12 g, 9.14 mmol) by an analogous procedure to that described in example 1. LC-MS (m/z) 384 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211901B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-5e407bdb07834375a9e0e97c3d211c88 |
| Source note | uspto-grants-2012_07 |