HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Cyanobenzoic acid → HCID 59590556, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Cyanobenzoic acid | HCID 12087 | — |
| Reactant | 4-Fluorobenzene-1,2-diamine | HCID 164584 | — |
| Product | HCID 59590556 | HCID 59590556 | 72% |
Reaction Steps
The title compound (186 mg, 72% yield) was prepared as a brown solid from 4-cyano-benzoic acid (294 mg, 2 mmol) and 4-fluoro-o-phenylenediamine (302 mg, 2.4 mmol) by an analogous procedure to that described in example 8. LC-MS (m/z) 260 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211901B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-b87f6e6ddecf4d26b2e7d2b7ea15dd2b |
| Source note | uspto-grants-2012_07 |