HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-Phenylenediamine → 3-(aminomethyl)-N-(2-aminophenyl)benzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | 3-Cyanobenzoic acid | HCID 15875 | — |
| Product | 3-(aminomethyl)-N-(2-aminophenyl)benzamide | HCID 59590553 | 58% |
Reaction Steps
The title compound (140 mg, 58% yield) was prepared as a grey solid from 3-cyano-benzoic acid (294 mg, 2 mmol) and o-phenylenediamine (432 mg, 4 mmol) by an analogous procedure to that described in example 8. LC-MS (m/z) 242 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08211901B2 |
| Source dataset | uspto-grants-2012_07 |
| ORD ID | ord-3f89adb50753470e9e841cc32739b418 |
| Source note | uspto-grants-2012_07 |