HCID 66920468, compound → HCID 66920521, compound

Participants

Reaction Steps

The compound of example 22, step 4 (66.0 mg, 124 μmol) was dissolved in ethanol (5 ml), and palladium on activated carbon (20 mg, 10%) was added. The mixture was hydrogenated overnight at room temperature and a hydrogen pressure of 4.5 bar. The mixture was filtered over celite and evaporated under reduced pressure to give 65.0 mg of the crude title compound.

Provenance & Evidence