Carbon Tetrachloride → HCID 66790033, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of (2-fluoro-5-{[(1R)-1-methylpropyl]oxy}phenyl)methanol (0.091 g, 0.459 mmol) in carbon tetrachloride (4.59 ml) was added triphenylphosphine resin (0.241 g, 0.918 mmol). The reaction was heated to 78° C. overnight in a pressure tube with minimal stirring. The reaction mixture was filtered through a fritted funnel and washed with carbon tetrachloride. The filtrate was concentrated to give the desired product.

Provenance & Evidence