Hydrogen Peroxide → HCID 69229766, compound

Participants

Reaction Steps

With reference to FIG. 8, general procedure II was used. The quantities of the chemicals in order of addition are as follows: NaBH4 (0.116 g, 3.08 mmol), THF (20 ml), BF3-ether complex (0.4 ml, 3.265 mmol), (R)-2-(4-(2-(benzhydryloxy)ethyl)-5,6-dihydropyridin-1(2H)-yl)-1-phenylethyl acetate 7a (0.7 g, 1.536 mmol), water (2 ml), ethanol (2 ml), 3N NaOH (1.1 ml) and 30% H2O2 (0.8 ml, 7.68 mmol).

Provenance & Evidence