反应详情

温度

65 °C

700.0 mg (2.67 mmol) N-[3-methyl-4-(morpholin-4-yl-carbonyl)-phenyl]-acetamide are combined with 7 ml 4-molar sodium hydroxide solution and stirred overnight at 65° C. The reaction mixture is poured onto ice water and extracted with ethyl acetate. The organic phase is dried over magnesium sulphate and evaporated down i. vac.

1. additionThe reaction mixture is poured onto ice water
2. extractionextracted with ethyl acetate
3. dry with materialThe organic phase is dried over magnesium sulphate
4. customevaporated down i