HRID1511175

反应详情

EQUATION

反应方程式

HRID 1511175 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

In another preparation, a 5.00 g sample of fluoxetine HCl and 0.85 g of succinic acid were dissolved in acetonitrile with heating. The solution was allowed to crystallize in an open evaporating dish over a 15 minute period. The solid material was isolated on filter paper and dried to yield 5.40 g (92% yield) of fluoxetine HCl:succinic acid (2:1) cocrystal.

WORKUP

后处理

  1. customIn another preparation
  2. temperaturewith heating
  3. customto crystallize in an open evaporating dish over a 15 minute period
  4. customThe solid material was isolated
  5. filtrationon filter paper
  6. customdried