Methyl cyclohexanecarboxylate → N-({[1-(But-3-en-1-yl)cyclohexyl]methoxy}carbonyl)-3-methyl-L-valine

Beteiligte Stoffe

Rolle	Name	HCID	Einwaage
Edukt	Methyl cyclohexanecarboxylate	HCID 20748	—
Edukt	(S)-2-((((2,2-Dimethylhex-5-en-1-yl)oxy)carbonyl)amino)-3,3-dimethylbutanoic acid	HCID 45379499	—
Produkt	N-({[1-(But-3-en-1-yl)cyclohexyl]methoxy}carbonyl)-3-methyl-L-valine	HCID 45379503	—

Reaktionsschritte

N-{[(1-But-3-en-1-ylcyclohexyl)methoxy]carbonyl}-3-methyl-L-valine was prepared according to the procedure for N-{[(2,2-dimethylhex-5-enyl)oxy]carbonyl}-3-methyl-L-valine by using methyl cyclohexanecarboxylate instead of ethyl isobutyrate in Step 1. LRMS (ESI) m/z 326.3 [(M+H)+; calcd for C18H32NO4: 326.2].

Herkunft & Nachweise

DOI	10.6084/m9.figshare.5104873.v1
Patentnummer	US08216999B2
Quelldatensatz	uspto-grants-2012_07
ORD ID	ord-557ceca2dc89454ca7dc13e5dca429a8
Quellennotiz	uspto-grants-2012_07