HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Methyl cyclopentanecarboxylate → N-({[1-(But-3-en-1-yl)cyclopentyl]methoxy}carbonyl)-3-methyl-L-valine
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Methyl cyclopentanecarboxylate | HCID 78365 | — |
| Edukt | (S)-2-((((2,2-Dimethylhex-5-en-1-yl)oxy)carbonyl)amino)-3,3-dimethylbutanoic acid | HCID 45379499 | — |
| Produkt | N-({[1-(But-3-en-1-yl)cyclopentyl]methoxy}carbonyl)-3-methyl-L-valine | HCID 45379502 | — |
Reaktionsschritte
N-{[(1-But-3-en-1-ylcyclopentyl)methoxy]carbonyl}-3-methyl-L-valine was prepared according to the procedure for N-{[(2,2-dimethylhex-5-enyl)oxy]carbonyl}-3-methyl-L-valine by using methyl cyclopentanecarboxylate instead of ethyl isobutyrate in Step 1. LRMS (ESI) m/z 312.3 [(M+H)+; calcd for C17H30NO4: 312.2].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08216999B2 |
| Quelldatensatz | uspto-grants-2012_07 |
| ORD ID | ord-b2a24cfce2dd47f29c93289d44d036f4 |
| Quellennotiz | uspto-grants-2012_07 |