HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2,2-Dimethylhex-5-en-1-ol → (2S)-({[(2,2-Dimethylhex-5-en-1-yl)oxy]carbonyl}amino)(1-methylcyclohexyl)acetic acid
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2,2-Dimethylhex-5-en-1-ol | HCID 10240821 | — |
| Edukt | 3-Methyl-N-{[(pent-4-en-1-yl)oxy]carbonyl}-L-valine | HCID 45379928 | — |
| Edukt | (S)-2-Amino-2-(1-methylcyclohexyl)acetic acid hydrochloride | HCID 57462912 | — |
| Produkt | (2S)-({[(2,2-Dimethylhex-5-en-1-yl)oxy]carbonyl}amino)(1-methylcyclohexyl)acetic acid | HCID 45379613 | — |
Reaktionsschritte
(2S)-({[(2,2-Dimethylhex-5-en-1-yl)oxy]carbonyl}amino)(1-methylcyclohexyl)acetic acid was prepared according to the procedure for 3-methyl-N-[(pent-4-enyloxy)carbonyl]-L-valine using (2S)-amino(1-methylcyclohexyl)acetic acid-HCl and 2,2-dimethylhex-5-en-1-ol. LRMS (ESI) m/z 326.3 [(M+H)+; calcd for C18H32NO4: 326.2].
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US08216999B2 |
| Quelldatensatz | uspto-grants-2012_07 |
| ORD ID | ord-5683f704c6584a37a2ce6346ec4ca42e |
| Quellennotiz | uspto-grants-2012_07 |